huagongshe.com
HRID44376

反应详情

EQUATION

反应方程式

HRID 44376 的结构方程式

REACTANTS

反应物

2
结构：NC(N)=S
HCID2723790

Thiourea

CH4N2S

结构：CN(C)c1nc(Cl)nc2ccccc12
HCID12684342

2-Chloro-N,N-dimethylquinazolin-4-amine

C10H10ClN3

PRODUCTS

生成物

1
结构：CN(C)c1nc(=S)[nH]c2ccccc12
HCID25222914

未命名化合物

PROCEDURE

实验过程

Prepared as in Example 46 from 2-chloro-N,N-dimethylquinazolin-4-amine (Example 40) and thiourea. 1H NMR (400 MHz, DMSO-d6) δ3.31 (s, 6H), 7.24-7.19 (m, 1H), 7.40-7.38 (m, 1H), 7.65-7.61 (m, 1H), 8.00 (d, J=8.0 Hz, 1H), 12.35 (s, 1H). MS 206 (MH+).