HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → N,N-diisopropyl-4-nitro-2-trichloromethylphenylsulfenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N,N-diisopropyl-4-nitro-2-trichloromethylphenylsulfenamide | HCID 23465374 | 95% |
Reaction Steps
A solution of 40 g of diisopropylamine in 400 ml of ether is placed in a stirred apparatus; at 10° C., 61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride in 200 ml of ether is dripped in. After the mixture has been reacted for 4 hours at 25° C., it is filtered and concentrated. There is obtained 70 g (95% of theory) of N,N-diisopropyl-4-nitro-2-trichloromethylphenylsulfenamide; m.p.: 104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04261924 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-27771e83846b4c428b9c07b595b008e5 |
| Source note | uspto-grants-1981_04 |