HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → N-allyl-4-nitro-2-trichloromethylphenylsulfenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Product | N-allyl-4-nitro-2-trichloromethylphenylsulfenamide | HCID 23465393 | 95% |
Reaction Steps
As in Example 4, 61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride is reacted with 23 g of allylamine. The hydrochloride is filtered off and the ether phase is concentrated. There is obtained 62 g (95% of theory) of N-allyl-4-nitro-2-trichloromethylphenylsulfenamide as a pale oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04261924 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-6e3c06f0d8a24476a4061dc20e4e31d1 |
| Source note | uspto-grants-1981_04 |