HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 443897Generated: October 30, 2026
Diethyl (ethoxymethylene)malonate → HCID 12892053, compound
https://huagongshe.com/reaction/443897
Participants
| Role | Name | HCID | Charge |
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| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | HCID 20514572 | HCID 20514572 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12892053 | HCID 12892053 | 95% |
Reaction Steps
A mixture of 5.5 parts of imidazo[2,1-b]benzothiazol-6-amine and 7.5 parts of diethyl 2-(ethoxymethylene)propanedioate is stirred for 30 minutes at 110° C. The solid product is suspended in 1,1'-oxybisethane. It is filtered off and dried, yielding 10 parts (95%) of diethyl 2-[(2,3-dihydroimidazo[2,1-b]benzothiazol-6-yl)aminomethylene]propanedioate; mp. 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04262004 |
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| Source dataset | uspto-grants-1981_04 |
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| ORD ID | ord-3f8dc5b836334694938a0757683269ca |
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| Source note | uspto-grants-1981_04 |
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