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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 443897Generated: October 30, 2026

Diethyl (ethoxymethylene)malonate → HCID 12892053, compound

https://huagongshe.com/reaction/443897

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl (ethoxymethylene)malonateHCID 6871—
ReactantHCID 20514572HCID 20514572—
SolventDiethyl EtherHCID 3283—
ProductHCID 12892053HCID 1289205395%

Reaction Conditions

Temperature110 °C

Reaction Steps

A mixture of 5.5 parts of imidazo[2,1-b]benzothiazol-6-amine and 7.5 parts of diethyl 2-(ethoxymethylene)propanedioate is stirred for 30 minutes at 110° C. The solid product is suspended in 1,1'-oxybisethane. It is filtered off and dried, yielding 10 parts (95%) of diethyl 2-[(2,3-dihydroimidazo[2,1-b]benzothiazol-6-yl)aminomethylene]propanedioate; mp. 140° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04262004
Source datasetuspto-grants-1981_04
ORD IDord-3f8dc5b836334694938a0757683269ca
Source noteuspto-grants-1981_04