Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → H-(D)Ala-Gly-OBzl.hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Boc-(D)Ala-Gly-OBzl | HCID 15567200 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | H-(D)Ala-Gly-OBzl.hydrochloride | HCID 131712174 | — |
반응 단계
3.4 g of Boc-(D)Ala-Gly-OBzl are dissolved in 50 ml of dioxane containing HCl and left to stand for one hour. The volume of the solution is reduced under vacuum and an excess of ether added. The precipitated salt is filtered off, dried and used as such for the coupling reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04261888 |
| 출처 데이터셋 | uspto-grants-1981_04 |
| ORD ID | ord-bde701a623bf43e4a1e85e704975ba84 |
| 출처 메모 | uspto-grants-1981_04 |