HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 54152476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | HCID 57147667 | HCID 57147667 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | HCID 54152476 | HCID 54152476 | — |
Reaction Steps
Using 25.83 g of 6-(p-benzyloxyphenyl)-3-hexen-2-one, 11.3 ml of ethyl bromoacetate and 6.63 g of zinc, the reaction and the purification of the product were carried out according to the method described in Example I (a) affording 29.6 g of ethyl 3-hydroxy-3-methyl-7-(p-benzyloxyphenyl)-4-heptenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262013 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-9b2aa49083734682a45a8537d386963e |
| Source note | uspto-grants-1981_04 |