HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 53696458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 3,5-Hexadien-2-one, 3-methyl-6-phenyl- | HCID 86886 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | HCID 53696458 | HCID 53696458 | — |
Reaction Steps
Using 8.60 g of 3-methyl-6-phenyl-3,5-hexadien-2-one, 8.0 ml of ethyl bromoacetate and 4.60 g of zinc, the reaction and the purification of the product were carried out according to the method described in Example 1 (a) affording 12.20 g of ethyl 3-hydroxy-3,4-dimethyl-7-phenyl-4,6-heptadienoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262013 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-74a9f1fcd11946cf8de781e01d8e1df2 |
| Source note | uspto-grants-1981_04 |