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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 443947Generated: October 30, 2026

Ethyl bromoacetate → HCID 54430174, compound

https://huagongshe.com/reaction/443947

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl bromoacetateHCID 7748—
ReactantHCID 57270480HCID 57270480—
CatalystZincHCID 23994—
ProductHCID 54430174HCID 5443017494.4%

Reaction Steps

Using 900 mg of 6-[p-(p-fluorobenzyloxy)phenyl]-3-hexen-2-one, 660 mg of ethyl bromoacetate and 260 mg of zinc, the reaction and the purification of the product were carried out according to the method described in Example 1 (a) affording 1.10 g of ethyl 3-hydroxy-3-methyl-7-[p-(p-fluorobenzyloxy)phenyl]-4-heptenoate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04262013
Source datasetuspto-grants-1981_04
ORD IDord-34d2b09b414f4423b8313ceddb2fbe39
Source noteuspto-grants-1981_04