HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl fluorosulfate → HCID 12495500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | 3-Methoxy-1,2-thiazole | HCID 12393928 | — |
| Product | HCID 12495500 | HCID 12495500 | 89% |
Reaction Steps
Methyl fluorosulfonate (6 ml) was added dropwise to 5.4 g (0.046 mol) of 3-methoxyisothiazole (exothermic reaction). After stirring for 30 min., the resulting solid was washed with ether to yield 9.3 g (89%) of 3-methoxy-2-methylisothiazolium fluorosulfonate, mp 120°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262127 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-90b1ee2fb6dd4ba7805d9c5370727192 |
| Source note | uspto-grants-1981_04 |