HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl fluorosulfate → HCID 86737693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | HCID 23466280 | HCID 23466280 | — |
| Product | HCID 86737693 | HCID 86737693 | 89% |
Reaction Steps
3-Allyloxyisothiazole (4.0 g, 0.028 mol) and 5 ml methyl fluorosulfonate were heated at 60° for 45 min. After cooling, the solid was washed with ether to yield 6.5 g (89%) of 3-allyloxy-2-methylisothiazolium fluorosulfonate, mp 50°-53°. Spectral data (NMR & IR) were consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262127 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-f0b692a4460f401d970a594f8caa7bd4 |
| Source note | uspto-grants-1981_04 |