HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl fluorosulfate → 3-Benzyloxy-2-methylisothiazolium fluorosulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | 3-Benzyloxyisothiazole | HCID 11183120 | — |
| Product | 3-Benzyloxy-2-methylisothiazolium fluorosulfonate | HCID 86737696 | 90% |
Reaction Steps
3-Benzyloxyisothiazole (3.0 g, 0.016 mol) and 5 ml of methyl fluorosulfonate were heated at 60° for 30 min. After cooling, the solid was washed with ether to yield 4.3 g (90%) of 3-benzyloxy-2-methylisothiazolium fluorosulfonate, mp 75°-78° C. (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262127 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-694570ea7a62452b888911aed976a17d |
| Source note | uspto-grants-1981_04 |