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HRID444036

反应详情

EQUATION

反应方程式

HRID 444036 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)N[N+](=O)[O-]
HCID62372

Nitrourea

CH3N3O3

结构：C=CC(=O)C=C
HCID543199

1,4-Pentadien-3-one

C5H6O

结构：CCOC(=O)CCCCCCC(NCCC(=O)c1ccccc1-c1ccccc1)C(=O)OCC
HCID70578184

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CCCCCCC(NCCC(O)c1ccccc1-c1ccccc1)C(=O)OCC
HCID70510532

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A solution of diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate (5 g), which was prepared via diethyl 2-(3-oxo-3-(p-biphenylyl)propylamino)nonanedioate from the appropriate vinyl ketone using the procedure of Example 2, in absolute ethanol (20 ml) was heated at 60° while nitrourea (1.12 g) was added portion-by-portion.

WORKUP

后处理

  1. additionwas added portion-by-portion