Dimethylamine → HCID 70567270, compound

HRID 444070Notes

Reaction equation

HRID 444070 reaction equation
[Cl:1][C:2]1[CH:22]=[CH:21][C:5]([O:6][C:7]2[CH:20]=[CH:19][C:10]([O:11][CH:12]([CH3:18])[CH:13]=[CH:14][C:15]([OH:17])=[O:16])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.[CH3:23][NH:24][CH3:25]>>[CH3:23][NH:24][CH3:25].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:6][C:7]2[CH:20]=[CH:19][C:10]([O:11][CH:12]([CH3:18])[CH:13]=[CH:14][C:15]([OH:17])=[O:16])=[CH:9][CH:8]=2)=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 53854823HCID 53854823, compound

Product 1

HCID 70567270HCID 70567270, compoundYield 92.2%

Procedure

In 15 ml of 10% dimethylamine aqueous solution, 7.0 g (0.02 mole) of 4-[4-(4-chlorophenoxy)phenoxy]2-pentenoic acid was dissolved and then, excess of dimethylamine and water was removed by a rotary evaporator to obtain 6.5 g of an orange viscous liquid, (yield: 92.2%).

Workup

  1. customexcess of dimethylamine and water was removed by a rotary evaporator

Sources & evidence

ORD record
ord-beae3c76630942279555b609691028b2
Source dataset
uspto-grants-1981_04
Patent number
US04263040

Reaction notes

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