HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 20536210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 5-Cyano-2,3-dihydro-3,3-dimethylbenzofuran-2-one | HCID 20536247 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20536210 | HCID 20536210 | — |
Reaction Steps
A suspension of 5-cyano-2,3-dihydro-3,3-dimethylbenzofuran-2-one (3.7 g), prepared as in Example 3, in diethyl ether (50 ml) was treated with a solution of dimethylamine in ethanol (8.6 ml of a 20.8% solution) portionwise with stirring at room temperature. The mixture was stirred for two hours, and the product was isolated by filtration, yield 4 g, mp 146°-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263037 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-3824eb102bb14d77a15bda92aa209d29 |
| Source note | uspto-grants-1981_04 |