HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2,3-Dihydro-3,3-dimethylbenzofuran-5-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,3-Dimethyl-2,3-dihydro-1-benzofuran-5-carboxylic acid | HCID 22041399 | — |
| Product | 2,3-Dihydro-3,3-dimethylbenzofuran-5-carboxylic acid chloride | HCID 54500736 | 127.7% |
Reaction Steps
The product of stage (a) (3 g) was boiled under reflux in thionyl chloride (3.6 g) for 3 hours. Removal of the thionyl chloride under vacuum gave crude title product (4.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263037 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-e892632284b0435a993f4e96d43c9caf |
| Source note | uspto-grants-1981_04 |