HCID 13013926, compound → HCID 23464495, compound

HRID 444160Notes

Reaction equation

HRID 444160 reaction equation
Cl[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[S:6][C:5]2[CH:13]=[C:14]([C:17]([O:19]C)=[O:18])[CH:15]=[CH:16][C:4]=2[N:3]=1.ClC1C2C=CC(C(OC)=O)=CC=2SC2C=CC=CC=2N=1>>[CH:9]1[C:8]2[CH:2]=[N:3][C:4]3[CH:16]=[CH:15][C:14]([C:17]([OH:19])=[O:18])=[CH:13][C:5]=3[S:6][C:7]=2[CH:12]=[CH:11][CH:10]=1

Participants

3

Procedure

Repeat the procedures of Examples 9 and 10, substituting an equivalent quantity of methyl 11-chlorodibenzo[b,f][1,4]thiazepin-7-carboxylate for the methyl 11-chlorodibenzo[b,f][1,4]thiazepin-3-carboxylate employed in Example 9, in order to obtain the title product.

Sources & evidence

ORD record
ord-4fa5a37b637042c3b927e660ee75bbc8
Source dataset
uspto-grants-1981_04
Patent number
US04263207

Reaction notes

Loading…