化工社化工社 化学情報印刷レポート · 研究参考用
Acetone → HCID 178479714、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | N-Phenylbenzimidoyl chloride | HCID 264587 | — |
| 反応物 | 2-[beta-(1-Pyrrolidinyl)ethylthio]phenol | HCID 23463674 | — |
| 生成物 | HCID 178479714 | HCID 178479714 | 55% |
反応手順
A solution of 5.5 gms (0.025 mole) of 2-[β-(1-pyrrolidinyl)ethylthio]phenol and 5.3 gms (0.025 mole) of N-phenylbenzimidoyl chloride in 50 ml acetone was stirred at room temperature for a period of two hours. The desired product crystallized out. It was filtered, washed with acetone and dried at room temperature. Recrystallization from isopropanol yielded 6.0 gms (55%) of product, M.P. 167°-9° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04264505 |
| 出典データセット | uspto-grants-1981_04 |
| ORD ID | ord-ab2aae96cb804d669c17c205bc8864e3 |
| 出典メモ | uspto-grants-1981_04 |