HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cholesterol → 1,4,6-Cholestatrien-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cholesterol | HCID 5997 | — |
| Reactant | 2,3-Dichloro-5,6-dicyano-1,4-benzoquinone | HCID 6775 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 1,4,6-Cholestatrien-3-one | HCID 107390 | 56% |
Reaction Steps
1,4,6-cholestatrien-3 one was prepared in 56% yield from cholesterol, 2,3-dichloro-5,6-dicyano-1,4-benzoquinone and dioxane by the procedure of A. B. Turner J. Chem. Soc. C, 2568 (1968).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04264512 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-783a3b8375f74c19a65838b24427a38f |
| Source note | uspto-grants-1981_04 |