HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59293668, compound → HCID 59293705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59293668 | HCID 59293668 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 59293705 | HCID 59293705 | — |
Reaction Steps
The title compound is prepared in analogy to the procedure described in Step 19.1 but using {5-[2-(2-dimethylamino-1,1-dimethyl-ethyl)-pyridin-4-yl]-4-methyl-thiazol-2-yl}-carbamic acid tert-butyl ester (Step 21.2) and stirring the reaction mixture for 2 h at rt. Title compound: ESI-MS: 291.1 [M+H]+; tR=2.48 min (System 1); TLC: Rf=0.11 (DCM/MeOH, 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476268B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-18bd16681c164f878df7e09f342ea46d |
| Source note | uspto-grants-2013_07 |