HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Chloroethyl)pyridine → HCID 57850232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Chloroethyl)pyridine | HCID 12481740 | — |
| Reactant | HCID 178492621 | HCID 178492621 | — |
| Product | HCID 57850232 | HCID 57850232 | — |
Reaction Steps
The title compound was prepared from 8-(2,5-dimethoxy-phenylsulfanyl)-9H-purin-6-ylamine and 4-(2-chloro-ethyl)-pyridine by a procedure similar to examples 1 and 2. The compound was purified by preparative HPLC. 1H NMR (CD3OD) δ 8.68 (d, J=6.4 Hz, 2H), 8.27 (s, 1H), 7.84 (d, J=6.4 Hz, 2H), 7.06-6.98 (m, 3H), 4.75 (t, J=6.8 Hz, 2H), 3.75 (s, 3H), 3.74 (s, 3H), 3.53 (t, J=6.8 Hz, 2H); LC-MS [M+H]+ 409.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476285B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-aa20f6f4a0524e7081c85b30309d9f74 |
| Source note | uspto-grants-2013_07 |