HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Bromoethyl)-3,5-bis(trifluoromethyl)benzene → HCID 57850798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Bromoethyl)-3,5-bis(trifluoromethyl)benzene | HCID 53402510 | — |
| Reactant | HCID 178508694 | HCID 178508694 | — |
| Product | HCID 57850798 | HCID 57850798 | — |
Reaction Steps
The title compound was prepared from 8-(6-bromo-benzo[1,3]dioxol-5-ylsulfanyl)-9H-purin-6-ylamine and 1-(2-bromo-ethyl)-3,5-bis-trifluoromethyl-benzene by a procedure similar to examples 1 and 2. The compound was purified by preparative HPLC. 1H NMR (DMSO-d6) δ 8.13 (s, 1H), 7.79 (s, 1H), 7.66 (s, 2H), 7.23 (s, 1H), 7.01 (s, 1H), 6.09 (s, 2H), 4.59 (t, J=7.4 Hz, 2H), 3.35 (t, J=7.4 Hz, 2H); LC-MS [M+H]+ 607.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476285B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-cb01388754cb4b05ab4f668690d1bdfc |
| Source note | uspto-grants-2013_07 |