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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 445072Generated: October 29, 2026

1-(2-Bromoethyl)-3,5-bis(trifluoromethyl)benzene → HCID 57850798, compound

https://huagongshe.com/reaction/445072

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2-Bromoethyl)-3,5-bis(trifluoromethyl)benzeneHCID 53402510—
ReactantHCID 178508694HCID 178508694—
ProductHCID 57850798HCID 57850798—

Reaction Steps

The title compound was prepared from 8-(6-bromo-benzo[1,3]dioxol-5-ylsulfanyl)-9H-purin-6-ylamine and 1-(2-bromo-ethyl)-3,5-bis-trifluoromethyl-benzene by a procedure similar to examples 1 and 2. The compound was purified by preparative HPLC. 1H NMR (DMSO-d6) δ 8.13 (s, 1H), 7.79 (s, 1H), 7.66 (s, 2H), 7.23 (s, 1H), 7.01 (s, 1H), 6.09 (s, 2H), 4.59 (t, J=7.4 Hz, 2H), 3.35 (t, J=7.4 Hz, 2H); LC-MS [M+H]+ 607.0

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08476285B2
Source datasetuspto-grants-2013_07
ORD IDord-cb01388754cb4b05ab4f668690d1bdfc
Source noteuspto-grants-2013_07