4-Bromo-3,5-dimethylphenol → HCID 67972414, compound

HRID 445112Notes

Reaction equation

HRID 445112 reaction equation
[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([OH:9])=[CH:4][C:3]=1[CH3:10].[Si:11]([O:18][CH2:19][CH2:20][CH2:21]Br)([C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:13])[CH3:12]>>[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([O:9][CH2:21][CH2:20][CH2:19][O:18][Si:11]([C:14]([CH3:15])([CH3:17])[CH3:16])([CH3:12])[CH3:13])=[CH:4][C:3]=1[CH3:10]

Participants

3

Reactant 2

HCID 819704-Bromo-3,5-dimethylphenolHCID 607486(3-Bromopropoxy)(tert-butyl)dimethylsilane

Product 1

HCID 67972414HCID 67972414, compoundYield 102.3%

Procedure

According to the method of (Example 17) <Step 1>, from 4-bromo-3,5-dimethylphenol (4.00 g) and 3-((tert-butyldimethylsilyl)oxy)propyl bromide (5.55 g), the subject compound (7.60 g) was obtained as a colorless oil.

Sources & evidence

ORD record
ord-048e762a4eba4bf28b6e98cf311822c5
Source dataset
uspto-grants-2013_07
Patent number
US08476287B2

Reaction notes

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