3-Bromobenzyl alcohol → HCID 67972468, compound

HRID 445119Notes

Reaction equation

HRID 445119 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH2:8][OH:9])[CH:5]=[CH:6][CH:7]=1.O[CH2:11][C:12]1[CH:17]=[CH:16][C:15]([B:18]([OH:20])[OH:19])=[CH:14][CH:13]=1>>[Br:1][C:2]1[CH:3]=[C:4]([CH2:8][O:9][CH2:11][C:12]2[CH:17]=[CH:16][C:15]([B:18]([OH:20])[OH:19])=[CH:14][CH:13]=2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 851413-Bromobenzyl alcoholHCID 27347064-(Hydroxymethyl)benzeneboronic acid

Product 1

HCID 67972468HCID 67972468, compound

Procedure

According to the method of (Example 129) <Step 1>, from (3-bromophenyl)methanol (0.50 g) and (4-(hydroxymethyl)phenyl)boronic acid (0.69), the subject compound (0.25 g) was obtained as a colorless solid.

Sources & evidence

ORD record
ord-85759f0ab0cc4fe7aa8fe4de6d076ab6
Source dataset
uspto-grants-2013_07
Patent number
US08476287B2

Reaction notes

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