Diethyl Ether → HCID 67307925, compound

Participants

Reaction Steps

Add a solution of hydrogen dichloride in ether (1 M, 122 μL, 122.0 μmol) to a solution of 4-(6-hydroxy-1-(4-(2-(piperidin-1-yl)ethoxy)phenoxy)naphthalen-2-yl)thiophene-3-carbonitrile (52 mg, 110.5 μmol) and dichloromethane (4 mL). Sonicate the mixture 5 minutes and then concentrate to obtain the title compound (57 mg, 110.5 μmol). MS (m/z): 471 (M+1-HCl).

Provenance & Evidence