Methanol → HCID 67285881, compound

Participants

Reaction Conditions

Reaction Steps

The compound (102 mg) obtained in Example 5(1) was dissolved in methanol (1 mL) and, furthermore, thionyl chloride (0.25 mL) was added at 0° C. The reaction solution was stirred at 60° C. for 1 hour. The reaction solution was concentrated under reduced pressure and the residue was purified by silica gel chromatography (manufactured by Fuji Silysia Chemical Ltd., CHROMATOREX NH (trade name)) (dichloromethane:methanol=1:0→4:1) to obtain the title compound (96.4 mg) having the following physical properties.

Provenance & Evidence