Diisopropylethylamine → HCID 59536373, compound

Participants

Reaction Steps

A solution of 1-(4-(trifluoromethyl)phenyl)-1,2,3,4-tetrahydroisoquinoline (97 mg, 0.350 mmol, example 9 (step 3), DIEA (61 μL, 0.35 mmol), and 3-iso-cyanatopyridine (42 mg, 0.35 mmol) in DCM (1 mL) was stirred at RT for 16 h. A white precipitate was observed. The reaction mixture was then filtered and the solid was dried in vacuo to give the title compound as a white solid. MS (ESI, positive ion) m/z: 398 (M+H).

Provenance & Evidence