3-Chlorothiophenol → HCID 58022625, compound

HRID 445423Notes

Reaction equation

HRID 445423 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([SH:8])[CH:5]=[CH:6][CH:7]=1.[Cl:9][C:10]1[CH:17]=[C:16](F)[CH:15]=[CH:14][C:11]=1[CH:12]=[O:13]>>[Cl:9][C:10]1[CH:17]=[C:16]([S:8][C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=2)[CH:15]=[CH:14][C:11]=1[CH:12]=[O:13]

Participants

3

Procedure

3-Chlorobenzenethiol and 2-chloro-4-fluorobenzaldehyde were reacted according to the same experiment procedures as in Reference Example 1 of the pamphlet of WO 03029205 to obtain the target product as a colorless oil.

Sources & evidence

ORD record
ord-a5d182d388e34765976912055ec0d1f1
Source dataset
uspto-grants-2013_07
Patent number
US08476305B2

Reaction notes

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