HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 14155580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1-benzyl-1,2,3,4-tetrahydroquinoline | HCID 12288350 | — |
| Product | HCID 14155580 | HCID 14155580 | — |
Reaction Steps
The procedure was carried out as described previously in step (a) of Example 5 with Compound 5 (0.42 g, 1.88 mmol), POCl3 (355 μL, 3.76 mmol), and DMF (3.5 mL). Compound 6 was obtained (0.36 g) as a viscous liquid and used without any further purification. The structure of Compound 6 is given below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476443B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-987735827bdc4cc3b3267fb78f3275ed |
| Source note | uspto-grants-2013_07 |