HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloroformate → HCID 68861352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | HCID 68861743 | HCID 68861743 | — |
| Product | HCID 68861352 | HCID 68861352 | — |
Reaction Steps
The procedure of Reference Example 2 was repeated by using the thus synthesized methyl (3R*,4S*)-1-benzyl-3,4-dimethylpyrrolidine-3-carboxylate crude product (12.28 g) and benzyl chloroformate (21.3 mL, 149.3 mmol) to obtain 4.23 g (14.52 mmol, 2 steps, 15%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476429B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-603f2ad69cf44c37833e1bbcb4fc4922 |
| Source note | uspto-grants-2013_07 |