HCID 86663436, compound → HCID 86663435, compound

Participants

Reaction Steps

A solution of the compound (162 mg, 0.461 mmol) obtained in Example 28c in methanol (5 mL) was added to 10% palladium-carbon (dry; 16 mg), and the atmosphere in the system was replaced with a hydrogen atmosphere, and then the mixture was stirred at room temperature for 1.5 hours. The atmosphere in the system was replaced with a nitrogen atmosphere, and the mixture was filtered through celite. The solvent was evaporated under reduced pressure to give the title compound (150 mg; yield, 100%) as a colorless oily substance.

Provenance & Evidence