HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 4-amino-, 1,1-dimethylethyl ester → HCID 66793868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 4-amino-, 1,1-dimethylethyl ester | HCID 233272 | — |
| Reactant | HCID 66671664 | HCID 66671664 | — |
| Product | HCID 66793868 | HCID 66793868 | 77.3% |
Reaction Steps
The compound (242 mg, 0.534 mmol) obtained in Example 31a was used to give a crude aldehyde compound (252 mg) according to the method described in Example 4g. The resulting crude aldehyde compound and tert-butyl 4-aminobenzoate (92 mg, 0.475 mmol) were used to give the title compound (231 mg; yield, 69%) as a white solid according to the method described in Example 18b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476253B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d54410a33034469da26fc16ff23e5131 |
| Source note | uspto-grants-2013_07 |