HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66797945, compound → HCID 66797906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66797945 | HCID 66797945 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 66797906 | HCID 66797906 | — |
Reaction Steps
The title compound was prepared following the procedure described in Example 3d using N-[(1R,3S,4S)-3-{[tert-butyl(dimethyl)silyl]oxy}-4-({[tert-butyl(dimethyl)-silyl]oxy}methyl)cyclopentyl]-6-(phenylethynyl)pyrimidin-4-amine and Pd(OH)2 on carbon (20% dry weight). LC/MS: Rt=2.30 min, ES+ 542 (FA standard).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481550B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-6771a5521c5249268b20a904e374a8d2 |
| Source note | uspto-grants-2013_07 |