反应详情

温度

118 °C

A suspension of 5-Amino-4,6-dichloropyrimidine (3 g, 0.02 mol) in ammonia (25 mL, 7N/MeOH, 0.175 mole) was heated at 118° C. overnight(under pressure). The reaction was cooled to 23° C., filtered and washed with ethanol to obtain 1.92 g (70%).

1. temperatureThe reaction was cooled to 23° C.
2. filtrationfiltered
3. washwashed with ethanol
4. customto obtain 1.92 g (70%)