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HRID44803

反应详情

EQUATION

反应方程式

HRID 44803 的结构方程式

REACTANTS

反应物

2
结构：NN
HCID9321

Hydrazine

H4N2

结构：CC[C@@H]1C(=O)N(C)c2cnc(Cl)nc2N1C1CCCC1
HCID24820413

(7R)-2-Chloro-8-cyclopentyl-7-ethyl-5-methyl-7,8-dihydropteridin-6(5H)-one

C14H19ClN4O

PRODUCTS

生成物

1
结构：CC[C@@H]1C(=O)N(C)c2cnc(NN)nc2N1C1CCCC1
HCID58405330

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Intermediate B and hydrazine (6 equivalents) in ethanol was heated in a microwave for 1 h at 120° C. The solvent was removed to give Intermediate B-2. This material was used without further purification.

WORKUP

后处理

  1. customThe solvent was removed
  2. customto give Intermediate B-2
  3. customThis material was used without further purification