HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Butylamino-1-cyclohexyloxy-2,2,6,6-tetramethylpiperidine → 1-Cyclohexyloxy-2,2,6,6-tetramethyl-1,2,3,6-tetrahydro-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Butylamino-1-cyclohexyloxy-2,2,6,6-tetramethylpiperidine | HCID 21182129 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Cyclohexyloxy-2,2,6,6-tetramethyl-1,2,3,6-tetrahydro-pyridine | HCID 57465186 | — |
Reaction Steps
Hydrogenation at this stage (MeOH, 5% Pd/C, 5 bar H2, 40° C.) leads to butyl-(1-cyclohexyloxy-2,2,6,6-tetramethyl-piperidin-4-yl)-amine, compound D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481726B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-043308aa0dd744cb9cb7c7cf7e004136 |
| Source note | uspto-grants-2013_07 |