HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aminoacetaldehyde dimethyl acetal → 7-Bromo-6-methylisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Reactant | 3-Bromo-4-methylbenzaldehyde | HCID 816765 | — |
| Product | 7-Bromo-6-methylisoquinoline | HCID 59496589 | — |
Reaction Steps
This compound was prepared by using procedures analogous to those described for the synthesis of Example 75, Step 1 starting from 3-bromo-4-methylbenzaldehyde (Aldrich, Cat. #4017458) and. aminoacetaldehyde dimethyl acetal. Analytic LCMS (M+H)+: m/z=221.95/223.95.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481732B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-66fcfe8a5a6d463f9b6baa757d41bd3f |
| Source note | uspto-grants-2013_07 |