Nitric Acid → Sulfuric acid, mixt. with nitric acid
Reaction equation
[S:1](=[O:5])(=[O:4])([OH:3])[OH:2].[N+:6]([O-:9])([OH:8])=[O:7]>>[S:1](=[O:3])(=[O:2])([OH:5])[OH:4].[N+:6]([O-:9])([OH:8])=[O:7]Participants
3
Procedure
Preferably, the batch process reaction mixture is formed by steps of: (i) premixing the sulfuric acid, nitric acid, and a graphite together to give a first sulfuric acid/nitric acid/graphite mixture; and (ii) adding the chlorate salt to the sulfuric acid/nitric acid/graphite mixture to give the reaction mixture. More preferably, the reaction mixture is formed by steps of: (i) premixing the sulfuric acid and nitric acid together to give a sulfuric acid/nitric acid mixture; (ii) adding a graphite to the sulfuric acid/nitric acid mixture to give a second sulfuric acid/nitric acid/graphite mixture; and (iii) adding a chlorate salt to the second sulfuric acid/nitric acid/graphite mixture to give the reaction mixture.
Sources & evidence
- ORD record
- ord-58225445a33947289636d2e41e9515e1
- Source dataset
- uspto-grants-2013_07
- Patent number
- US08486302B2
Reaction notes
Loading…