Isopropanol → HCID 58554766, compound

Participants

Reaction Steps

10% Palladium on charcoal (0.140 g) was added in one portion to a stirred solution of 24 (0.70 g, 1.02 mmol) in 1:1 mixture of isopropanol (10 mL) and THF (10 mL) under nitrogen atmosphere. The suspension was then stirred under hydrogen atmosphere at room temperature for 4 h. The solution was filtered through celite and concentrated under reduced pressure to obtain (S)-5-(2-(4-aminobenzoyloxy)ethoxy)-2-(9H-carbazol-9-yl)-5-oxopentanoic acid 25 (0.45 g, 96%) as a white solid.

Provenance & Evidence