1,3-Bis(dibenzylphosphonooxy)-4-cyclohexylbenzene → HCID 54597260, compound

Participants

Reaction Steps

To an ethanol solution (10 ml) of 1,3-bis(dibenzylphosphonooxy)-4-cyclohexylbenzene (1.75 g), 5% palladium-carbon (50% water-containing product) (256 mg) was added and stirred under a hydrogen atmosphere at room temperature for 14 hours. After the removal of the catalyst by filtration, the filtrate was concentrated, to give the light yellow title compound (805 mg, yield: 93%).

Provenance & Evidence