Tributylstannane → HCID 90910115, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of tert-butyl 2,2-dichlorocyclopropanecarboxylate (1.0 g, 4.7 mmol), tributyltin hydride (1.68 g, 5.7 mmol) and AIBN (50 mg) were heated to 90° C. for 1 h. The mixture was cooled to room temperature and distillation afforded a mixture of cis and trans t-butyl 2-chloro-1-cyclopropane carboxylate (220 mg, yield: 26%).

Provenance & Evidence