HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 2-Methoxy-5-nitro-benzoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 2-Methoxy-5-nitrobenzoic acid | HCID 284163 | — |
| Produkt | 2-Methoxy-5-nitro-benzoyl chloride | HCID 13719593 | 100% |
Reaktionsschritte
2-Methoxy-5-nitro benzoic acid (500 mg, 2.5 mmol) was heated to reflux with thionyl chloride (5 ml) for 4 hr. The excess thionyl chloride was evaporated under reduced pressure to yield 2-methoxy-5-nitro-benzoyl chloride (0.55 g, 100%), which was used as such for the next step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08486962B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-89712d9cf5fb49ef82ff311ba6bb831c |
| Quellennotiz | uspto-grants-2013_07 |