[(1S)-1-(5-fluoropyridin-2-yl)propyl]amine → HCID 178466926, compound

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Reaction Steps

The title compound was prepared using a procedure similar to the one described for the synthesis of Intermediate 28 using 6-chloro-N-(5-ethoxy-1H-pyrazol-3-yl)-3-nitropyridin-2-amine (Intermediate 26) and [(1S)-1-(5-fluoropyridin-2-yl)propyl]amine (Intermediate 35) as the starting materials. LCMS: 402 [M+1]. 1H NMR (400 MHz, DMSO-d6) δ 12.00 (s, 1H), 11.00 (s, 1H), 8.80 (s, 1H), 8.50 (s, 1H), 8.10 (d, 1H), 7.60 (m, 1H), 7.20 (m, 1H), 6.30 (m, 1H), 5.80 (s, 1H), 5.00 (m, 1H), 4.10 (q, 2H), 2.00 (m, 2H), 1.40 (d, 3H), 1.10 (t, 3H).

Provenance & Evidence