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HRID450596

反应详情

EQUATION

反应方程式

HRID 450596 的结构方程式

REACTANTS

反应物

3
结构：N
HCID222

Ammonia gas

H3N

结构：O=C(Cl)c1cccc(S(=O)(=O)C(F)(F)F)c1
HCID59819913

未命名化合物

结构：N=C(NO)c1cccnc1
HCID178513339

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(c1cccc(-c2nc(-c3cccnc3)no2)c1)C(F)(F)F
HCID67026134

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure of Example 1 using N-hydroxynicotinimidamide (Aldrich) and the compound of Example 6B. 1H NMR (300 MHz, DMSO-d6) δ 7.73 (dd, J=4, 5.0 Hz, 1 H), 7.85 (t, J=8 Hz, 1 H), 8.13 (m, 1 H), 8.43 (m, 1 H) 8.5 (m, 1 H), 8.6 (m, 1 H), 8.92 (m, 1 H), 9.37 (m, 1 H) ppm; MS (DCI/NH3) m/z 356 (M+H)+.