Ammonia → HCID 67026267, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 4-fluoro-3-hydroxybenzoic acid (Aldrich). 1H NMR (300 MHz, DMSO-d6) δ 7.45 (dd, J=11.1, 8.7 Hz, 1 H), 7.62-7.71 (m, 2 H), 7.78 (dd, J=8.3, 2.0 Hz, 1 H), 8.43 (dt, J=7.9, 1.8 Hz, 1 H), 8.82 (dd, J=5.0, 1.8 Hz, 1 H), 9.24 (d, J=2.0 Hz, 1 H) ppm; MS (DCI/NH3) m/z 258 (M+H)+.

Provenance & Evidence