HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 136360178, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Fluoro-4-hydroxybenzoic acid | HCID 160456 | — |
| Reactant | N-Hydroxynicotinimidamide | HCID 308113 | — |
| Product | HCID 136360178 | HCID 136360178 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 3-fluoro-4-hydroxybenzoic acid (Aldrich). 1H NMR (300 MHz, CD3OD) δ 7.09 (t, J=8.7 Hz, 1 H), 7.63 (ddd, J=7.9, 5.2, 0.8 Hz, 1 H), 7.86-7.93 (m, 2 H), 8.53 (dt, J=7.9, 2.0 Hz, 1 H), 8.72 (dd, J=4.8, 1.6 Hz, 1 H), 9.27 (dd, J=2.4, 0.8 Hz, 1 H) ppm; MS (DCI/NH3) m/z 258 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-8e7c8f4c14a64fa2bc54877f19290fbe |
| Source note | uspto-grants-2013_07 |