Ammonia → HCID 86621257, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 4-(2,2,2-trifluoroacetyl)benzoic acid (Aldrich). 1H NMR (300 MHz, CD3OD) δ 7.81 (ddd, J=7.9, 5.2, 0.8 Hz, 1 H), 7.96 (d, J=8.3 Hz, 2 H), 8.28 (d, J=8.7 Hz, 2 H), 8.76 (dt, J=8.2, 1.8 Hz, 1 H), 8.82 (dd, J=5.2, 1.6 Hz, 1 H), 9.38 (d, J=1.6 Hz, 1 H) ppm; MS (DCI/NH3) m/z 320 (M+H)+.

Provenance & Evidence