huagongshe.com
HRID450624

反应详情

EQUATION

反应方程式

HRID 450624 的结构方程式

REACTANTS

反应物

3
结构：N
HCID222

Ammonia gas

H3N

结构：NS(=O)(=O)c1cccc(C(=O)O)c1
HCID229352

3-sulfamoylbenzoic acid

C7H7NO4S

结构：NC(=NO)c1cccnc1
HCID308113

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cccc(-c2nc(-c3cccnc3)no2)c1
HCID59758743

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 3-sulfamoylbenzoic acid (Oakwood). 1H NMR (300 MHz, CD3OD) δ 7.65 (ddd, J=8.0, 4.9, 1.0 Hz, 1 H), 7.83 (t, J=7.9 Hz, 1 H), 8.21 (ddd, J=7.9, 1.8, 1.0 Hz, 1 H), 8.45 (dt, J=7.9, 1.4 Hz, 1 H), 8.58 (dt, J=8.0, 1.9 Hz, 1 H), 8.73-8.77 (m, 2 H), 9.31 (dd, J=2.2, 1.0 Hz, 1 H) ppm; MS (DCI/NH3) m/z 303 (M+H)+.