HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 30028912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N-Hydroxynicotinimidamide | HCID 308113 | — |
| Reactant | 2-Chloropyridine-4-carbonyl chloride | HCID 2800003 | — |
| Product | HCID 30028912 | HCID 30028912 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 1 using N′-hydroxynicotinimidamide (Aldrich) and 2-chloroisonicotinoyl chloride (Maybridge). 1H NMR (300 MHz, DMSO-d6) δ 7.68 (ddd, J=7.9, 4.8, 0.8 Hz, 1 H), 8.16 (dd, J=5.1, 1.4 Hz, 1 H), 8.23 (dd, J=1.5, 0.8 Hz, 1 H), 8.42-8.54 (m, 1 H), 8.77 (dd, J=5.1, 0.7 Hz, 1 H), 8.84 (dd, J=4.7, 1.7 Hz, 1 H), 9.28 (dd, J=2.2, 0.8 Hz, 1 H) ppm; MS (DCI/NH3) m/z 259 (M+H)+, 261 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-02ca28e78a674a168aa5da22cde31068 |
| Source note | uspto-grants-2013_07 |