HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 44544771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Pyrimidine-5-carboxylic acid | HCID 78346 | — |
| Reactant | N-Hydroxy-4-pyridazinecarboximidamide | HCID 136140373 | — |
| Product | HCID 44544771 | HCID 44544771 | — |
Reaction Steps
The titled compound was prepared according to the procedure of Method C using the product of Example 83D and pyrimidine-5-carboxylic acid (Maybridge). 1H NMR (300 MHz, CD3OD) δ 8.41 (dd, J=5.4, 2.4 Hz, 1 H), 9.44 (s, 1 H), 9.47 (dd, J=5.4, 1.4 Hz, 1 H), 9.59 (s, 2 H), 9.90 (dd, J=2.2, 1.2 Hz, 1 H) ppm; MS (DCI/NH3) m/z=227 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ec3c16376c1f48d39eac7c4b47b0b548 |
| Source note | uspto-grants-2013_07 |