HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178420781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N-Hydroxynicotinimidamide | HCID 308113 | — |
| Reactant | HCID 178524184 | HCID 178524184 | — |
| Product | HCID 178420781 | HCID 178420781 | — |
Reaction Steps
The title compound was prepared according to Method C using 1H-benzo[d][1,2,3]triazole-5-carboxylic acid (Aldrich) and N′-hydroxynicotinimidamide (Tyger). 1H NMR (300 MHz, DMSO-d6) δ 7.67 (ddd, J=8.0, 4.9, 0.7 Hz, 1 H), 8.10-8.20 (m, 1 H), 8.22-8.31 (m, 1 H), 8.49 (dt, J=8.1, 2.0, 1.7 Hz, 1 H), 8.75-8.92 (m, 2 H), 9.30 (dd, J=2.2, 0.8 Hz, 1 H) ppm; MS (DCI/NH3) m/z 265 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-09fc4d4d510d48c5a48809730b2af04e |
| Source note | uspto-grants-2013_07 |